Knowledge (XXG)

Bead test

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101:
The bead is allowed to cool and then wetted and dipped into the sample to be tested such that only a tiny amount of the substance adheres to the bead. If too much substance is used, the bead will become dark and opaque. The bead and adhering substance is then heated in the lower,
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wire and heated in a Bunsen burner flame until red hot. A stick made of another inert substance such as a magnesia stick (MgO) may also be used. It is then dipped into powdered
581: 635: 608: 35: 87: 137:. After the test, the bead is removed by heating it to fusion point, and plunging it into a vessel of water. 671: 106:, part of the flame, allowed to cool, and the colour observed. It is then heated in the upper, 631: 604: 91: 614: 597: 63: 55: 148: 107: 95: 59: 153: 103: 51: 665: 509: 90:
and then shrinks, forming a colourless, transparent glass-like bead (a mixture of
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and held in the hottest part of the flame where it swells up as it loses its
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Vogel's Textbook of Macro and Semimicro Qualitative Inorganic Analysis
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to test for the presence of certain metals. The oldest one is the
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Characteristic coloured beads are produced with salts of
596: 578:Materials Handbook: A Concise Desktop Reference 50:in 1812. Since then other salts were used as 8: 139: 62:. The most important one after borax is 590: 588: 573: 571: 567: 27:Test for the presence of certain metals 628:CRC Handbook of Chemistry and Physics 595:Vogel, Arthur I.; Svehla, G. (1979), 78:A small loop is made in the end of a 7: 413:yellow, opaque (hot) violet (cold) 384:yellow-brown (hot and cold), opaque 345:yellow-brown (hot and cold), opaque 306:yellow-brown (hot and cold), opaque 203:colorless, yellow or brownish (hot) 25: 603:(5th ed.), London: Longman, 410:colourless (hot and cold), opaque 319:colourless (hot and cold), opaque 540:colourless(hot and cold), opaque 527:colourless(hot and cold), opaque 514:colourless(hot and cold), opaque 501:colourless(hot and cold), opaque 488:colourless(hot and cold), opaque 475:colourless(hot and cold), opaque 462:colourless(hot and cold), opaque 449:colourless(hot and cold), opaque 436:colourless(hot and cold), opaque 423:colourless(hot and cold), opaque 397:colourless(hot and cold), opaque 371:colourless(hot and cold), opaque 332:colourless(hot and cold), opaque 293:deep blue (hot and cold), opaque 178:colorless, yellow or brown (hot) 165:colorless (hot and cold), opaque 254:sky blue (hot and cold), opaque 36:qualitative inorganic analysis 1: 267:yellow (hot and cold), opaque 358:green (hot and cold), opaque 66:, which is the basis of the 280:pink (hot and cold), opaque 688: 68:microcosmic salt bead test 244:colorless (hot and cold) 34:is a traditional part of 452:yellow or brown, opaque 88:water of crystallization 46:. It was introduced by 580:, François Cardarelli 270:bottle-green, opaque 630:. CRC Press. 1985. 543:colourless, opaque 530:colourless, opaque 517:colourless, opaque 504:colourless, opaque 491:colourless, opaque 478:colourless, opaque 465:colourless, opaque 439:colourless, opaque 400:colourless, opaque 652:"Borax Bead Tests" 296:deep blue, opaque 283:colorless, opaque 168:colorless, opaque 547: 546: 92:sodium metaborate 16:(Redirected from 679: 656: 655: 648: 642: 641: 624: 618: 617: 615:Internet Archive 613:– via the 602: 592: 583: 575: 219:gray and opaque 206:gray and opaque 181:gray and opaque 140: 64:microcosmic salt 56:sodium carbonate 21: 687: 686: 682: 681: 680: 678: 677: 676: 662: 661: 660: 659: 650: 649: 645: 638: 626: 625: 621: 611: 594: 593: 586: 576: 569: 564: 552: 149:Oxidizing flame 96:boric anhydride 76: 60:sodium fluoride 40:borax bead test 28: 23: 22: 18:Borax bead test 15: 12: 11: 5: 685: 683: 675: 674: 672:Chemical tests 664: 663: 658: 657: 643: 636: 619: 609: 584: 566: 565: 563: 560: 559: 558: 551: 548: 545: 544: 541: 538: 532: 531: 528: 525: 519: 518: 515: 512: 506: 505: 502: 499: 493: 492: 489: 486: 480: 479: 476: 473: 467: 466: 463: 460: 454: 453: 450: 447: 441: 440: 437: 434: 428: 427: 426:brown, opaque 424: 421: 415: 414: 411: 408: 402: 401: 398: 395: 389: 388: 385: 382: 376: 375: 372: 369: 363: 362: 361:green, opaque 359: 356: 350: 349: 348:green, opaque 346: 343: 337: 336: 335:green, opaque 333: 330: 324: 323: 320: 317: 311: 310: 307: 304: 298: 297: 294: 291: 285: 284: 281: 278: 272: 271: 268: 265: 259: 258: 255: 252: 246: 245: 242: 239: 233: 232: 230: 227: 221: 220: 217: 214: 208: 207: 204: 201: 195: 194: 192: 189: 183: 182: 179: 176: 170: 169: 166: 163: 157: 156: 154:Reducing flame 151: 146: 75: 72: 52:fluxing agents 26: 24: 14: 13: 10: 9: 6: 4: 3: 2: 684: 673: 670: 669: 667: 653: 647: 644: 639: 637:0-8493-0466-0 633: 629: 623: 620: 616: 612: 610:0-582-44367-9 606: 601: 600: 591: 589: 585: 582: 579: 574: 572: 568: 561: 557: 554: 553: 549: 542: 539: 537: 534: 533: 529: 526: 524: 521: 520: 516: 513: 511: 508: 507: 503: 500: 498: 495: 494: 490: 487: 485: 482: 481: 477: 474: 472: 469: 468: 464: 461: 459: 456: 455: 451: 448: 446: 443: 442: 438: 435: 433: 430: 429: 425: 422: 420: 417: 416: 412: 409: 407: 404: 403: 399: 396: 394: 391: 390: 387:grey, opaque 386: 383: 381: 378: 377: 374:grey, opaque 373: 370: 368: 365: 364: 360: 357: 355: 352: 351: 347: 344: 342: 339: 338: 334: 331: 329: 326: 325: 322:grey, opaque 321: 318: 316: 313: 312: 309:grey, opaque 308: 305: 303: 300: 299: 295: 292: 290: 287: 286: 282: 279: 277: 274: 273: 269: 266: 264: 261: 260: 256: 253: 251: 248: 247: 243: 240: 238: 235: 234: 231: 228: 226: 223: 222: 218: 215: 213: 210: 209: 205: 202: 200: 197: 196: 193: 190: 188: 185: 184: 180: 177: 175: 172: 171: 167: 164: 162: 159: 158: 155: 152: 150: 147: 145: 142: 141: 138: 136: 132: 128: 124: 120: 116: 111: 109: 105: 99: 97: 93: 89: 85: 81: 73: 71: 69: 65: 61: 57: 53: 49: 45: 41: 37: 33: 19: 646: 627: 622: 598: 577: 510:Praseodymium 257:red, opaque 112: 100: 77: 67: 44:blister test 43: 39: 31: 29: 562:References 556:Flame test 445:Molybdenum 74:Borax bead 54:, such as 536:Germanium 497:Neodymium 458:Strontium 432:Magnesium 276:Manganese 241:red (hot) 229:colorless 216:colorless 191:colorless 127:manganese 108:oxidizing 48:Berzelius 32:bead test 666:Category 550:See also 419:Tungsten 406:Titanium 367:Platinum 354:Chromium 328:Vanadium 174:Antimony 161:Aluminum 123:chromium 104:reducing 80:platinum 523:Silicon 484:Yttrium 471:Thorium 341:Uranium 225:Calcium 212:Cadmium 199:Bismuth 634:  607:  315:Silver 302:Nickel 289:Cobalt 250:Copper 237:Cerium 187:Barium 135:nickel 131:cobalt 115:copper 144:Metal 84:borax 632:ISBN 605:ISBN 380:Gold 263:Iron 133:and 119:iron 94:and 30:The 393:Tin 98:). 58:or 42:or 668:: 587:^ 570:^ 129:, 125:, 121:, 117:, 70:. 654:. 640:. 20:)

Index

Borax bead test
qualitative inorganic analysis
Berzelius
fluxing agents
sodium carbonate
sodium fluoride
microcosmic salt
platinum
borax
water of crystallization
sodium metaborate
boric anhydride
reducing
oxidizing
copper
iron
chromium
manganese
cobalt
nickel
Metal
Oxidizing flame
Reducing flame
Aluminum
Antimony
Barium
Bismuth
Cadmium
Calcium
Cerium

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