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Cryopump

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204:. Baffles are often attached to the cold head to expand the surface area available for condensation, but these also increase the radiative heat uptake of the cryopump. Over time, the surface eventually saturates with condensate and thus the pumping speed gradually drops to zero. It will hold the trapped gases as long as it remains cold, but it will not condense fresh gases from leaks or backstreaming until it is regenerated. Saturation happens very quickly in low vacuums, so cryopumps are usually only used in high or ultrahigh vacuum systems. 25: 211:
range. The cryopump operates on the principle that gases can be condensed and held at extremely low vapor pressures, achieving high speeds and throughputs. The cold head consists of a two-stage cold head cylinder (part of the vacuum vessel) and a drive unit displacer assembly. These together produce
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Regeneration of a cryopump is the process of evaporating the trapped gases. During a regeneration cycle, the cryopump is warmed to room temperature or higher, allowing trapped gases to change from a solid state to a gaseous state and thereby be released from the cryopump through a pressure relief
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Some cryopumps have multiple stages at various low temperatures, with the outer stages shielding the coldest inner stages. The outer stages condense high boiling point gases such as water and oil, thus saving the surface area and refrigeration capacity of the inner stages for lower boiling point
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As cooling temperatures decrease when using dry ice, liquid nitrogen, then compressed helium, lower molecular-weight gases can be trapped. Trapping nitrogen, helium, and hydrogen requires extremely low temperatures (~10K) and large surface area as described below. Even at this temperature, the
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Most production equipment utilizing a cryopump have a means to isolate the cryopump from the vacuum chamber so regeneration takes place without exposing the vacuum system to released gasses such as water vapor. Water vapor is the hardest natural element to remove from vacuum chamber walls upon
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by condensing them on a cold surface, but are only effective on some gases. The effectiveness depends on the freezing and boiling points of the gas relative to the cryopump's temperature. They are sometimes used to block particular contaminants, for example in front of a
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When regeneration is complete, the cryopump will be roughed to 50μm (50 milliTorr or μmHg), isolated, and the rate-of-rise (ROR) will be monitored to test for complete regeneration. If the ROR exceeds 10μm/min the cryopump will require additional purge time.
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to cool the pump, either in a large liquid helium reservoir, or by continuous flow into the cryopump. However, over time most cryopumps were redesigned to use gaseous helium, enabled by the invention of better
172:. In the 1970s, the Gifford-McMahon cryocooler was used to make a vacuum pump by Helix Technology Corporation and its subsidiary company Cryogenic Technology Inc. In 1976, cryopumps began to be used in 176:'s manufacturing of integrated circuits. The use of cryopumps became common in semiconductor manufacturing worldwide, with expansions such as a cryogenics company founded jointly by Helix and 267:
exposure to the atmosphere due to monolayer formation and hydrogen bonding. Adding heat to the dry nitrogen purge-gas will speed the warm-up and reduce the regeneration time.
128:). There is a delay between the molecule impinging on the surface and rebounding from it. Kinetic energy will have been lost as the molecules slow down. For example, 239:
saturates, the effectiveness of a sorption pump decreases, but can be recharged by heating the zeolite material (preferably under conditions of low pressure) to
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closed-cycle refrigeration at temperatures that range from 60 to 80K for the first-stage cold station to 10 to 20K for the second-stage cold station, typically.
136:, but it can be cryotrapped. This effectively traps molecules for an extended period and thereby removes them from the vacuum environment just like cryopumping. 243:
it. The breakdown temperature of the zeolite material's porous structure may limit the maximum temperature that it may be heated to for regeneration.
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Sorption pumps are a type of cryopump that is often used as roughing pumps to reduce pressures from the range of atmospheric to on the order of 0.1
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can also refer to a somewhat different effect, where molecules will increase their residence time on a cold surface without actually freezing (
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lighter gases helium and hydrogen have very low trapping efficiency and are the predominant molecules in ultra-high vacuum systems.
68: 46: 424:(2), Transactions of the Japan Society of Refrigerating and Air Conditioning Engineers, Volume 11, Issue 2, pp. 89-99: 89, 522: 160:. The key refrigeration technology was discovered in the 1950s by two employees of the Massachusetts-based company 363: 551: 39: 33: 517: 181: 50: 541: 451: 425: 413: 228: 499: 486: 503: 467: 344: 309: 165: 459: 336: 301: 161: 145: 197: 455: 429: 546: 491: 99: 535: 340: 247: 224: 152: 125: 103: 418:
Transactions of the Japan Society of Refrigerating and Air Conditioning Engineers
292:(1875). "4. Preliminary Note "On a New Method of obtaining very perfect Vacua". 289: 86: 305: 240: 201: 169: 157: 471: 348: 313: 192:
Cryopumps are commonly cooled by compressed helium, though they may also use
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An experimental investigation of pulse tube refrigeration heat pumping rate
250:(10 Torr), while lower pressures are achieved using a finishing pump (see 444:
Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films
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Bridwell, M. C.; Rodes, J. G. (1985). "History of the modern cryopump".
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The cryopump provides fast, clean pumping of all gases in the 10 to 10
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Baechler, Werner G. (1987). "Cryopumps for research and industry".
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by coating the cold head with highly adsorbing materials such as
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to keep out water. In this function, they are called a
498:(2nd ed.). New York: VCH Publisher. pp.  485: 200:, or stand-alone versions may include a built-in 144:Early experiments into cryotrapping of gasses in 300:. Cambridge University Press (CUP): 348–349. 294:Proceedings of the Royal Society of Edinburgh 8: 102:to trap backstreaming oil, or in front of a 382:Gifford, W. E.; Longsworth, R. C. (1965), 362:Gifford, W. E.; Longsworth, R. C. (1964), 168:. This technology came to be known as the 69:Learn how and when to remove this message 32:This article includes a list of general 484:Van Atta, C. M.; M. Hablanian (1991) . 450:(3). American Vacuum Society: 472–475. 280: 7: 526:. Bradley, IL: Lindsay Publications. 148:were conducted as far back as 1874. 371:, Trans. ASME, J. Eng. Ind. 63, 264 523:Procedures in Experimental Physics 223:Cryopumps are often combined with 38:it lacks sufficient corresponding 14: 151:The first cryopumps mainly used 23: 487:"Vacuums and Vacuum Technology" 1: 341:10.1016/0042-207x(87)90078-9 494:and George L. Trigg (ed.). 335:(1–2). Elsevier BV: 21–29. 263:valve into the atmosphere. 85:or a "cryogenic pump" is a 568: 412:Matsubara, Yoichi (1994), 401:, Adv. Cryog. Eng. 12, 608 397:Longsworth, R. C. (1967), 386:, Adv. Cryog. Eng. 11, 171 170:Gifford-McMahon cryocooler 414:"Pulse Tube Refrigerator" 306:10.1017/s0370164600029734 164:, William E. Gifford and 365:Pulse tube refrigeration 216:gases such as nitrogen. 496:Encyclopedia of Physics 132:does not condense at 8 53:more precise citations. 162:Arthur D. Little Inc. 384:Surface heat pumping 456:1985JVSTA...3..472B 430:2011TRACE..11...89M 16:Type of vacuum pump 229:activated charcoal 146:activated charcoal 166:Howard O. McMahon 79: 78: 71: 559: 552:Gas technologies 527: 513: 489: 476: 475: 464:10.1116/1.573017 439: 433: 432: 409: 403: 402: 394: 388: 387: 379: 373: 372: 370: 359: 353: 352: 324: 318: 317: 285: 74: 67: 63: 60: 54: 49:this article by 40:inline citations 27: 26: 19: 567: 566: 562: 561: 560: 558: 557: 556: 532: 531: 516: 510: 483: 480: 479: 441: 440: 436: 411: 410: 406: 396: 395: 391: 381: 380: 376: 368: 361: 360: 356: 326: 325: 321: 287: 286: 282: 277: 260: 198:liquid nitrogen 190: 142: 75: 64: 58: 55: 45:Please help to 44: 28: 24: 17: 12: 11: 5: 565: 563: 555: 554: 549: 544: 534: 533: 530: 529: 514: 508: 492:Rita G. Lerner 478: 477: 434: 404: 389: 374: 354: 319: 279: 278: 276: 273: 259: 256: 225:sorption pumps 189: 186: 141: 138: 100:diffusion pump 77: 76: 31: 29: 22: 15: 13: 10: 9: 6: 4: 3: 2: 564: 553: 550: 548: 545: 543: 540: 539: 537: 525: 524: 519: 515: 511: 509:0-89573-752-3 505: 501: 497: 493: 488: 482: 481: 473: 469: 465: 461: 457: 453: 449: 445: 438: 435: 431: 427: 423: 419: 415: 408: 405: 400: 393: 390: 385: 378: 375: 367: 366: 358: 355: 350: 346: 342: 338: 334: 330: 323: 320: 315: 311: 307: 303: 299: 295: 291: 288:Tait, P. G.; 284: 281: 274: 272: 268: 264: 257: 255: 253: 249: 244: 242: 238: 234: 230: 226: 221: 217: 213: 210: 205: 203: 199: 195: 187: 185: 183: 179: 175: 171: 167: 163: 159: 154: 153:liquid helium 149: 147: 139: 137: 135: 131: 127: 123: 119: 117: 113: 109: 105: 101: 96: 92: 88: 84: 73: 70: 62: 52: 48: 42: 41: 35: 30: 21: 20: 542:Vacuum pumps 521: 518:Strong, John 495: 490:. In Ed. by 447: 443: 437: 421: 417: 407: 398: 392: 383: 377: 364: 357: 332: 328: 322: 297: 293: 290:Dewar, James 283: 269: 265: 261: 258:Regeneration 245: 222: 218: 214: 206: 191: 150: 143: 126:supercooling 122:Cryotrapping 121: 120: 115: 111: 107: 104:McLeod gauge 82: 80: 65: 59:January 2013 56: 37: 528:, Chapter 3 184:) in 1981. 158:cryocoolers 89:that traps 87:vacuum pump 51:introducing 536:Categories 275:References 202:cryocooler 34:references 500:1330–1334 472:0734-2101 349:0042-207X 314:0370-1646 235:. As the 188:Operation 116:cold trap 112:waterpump 520:(1938). 182:jp:アルバック 130:hydrogen 108:cryotrap 83:cryopump 452:Bibcode 426:Bibcode 237:sorbent 233:zeolite 194:dry ice 140:History 134:kelvins 95:vapours 47:improve 506:  470:  347:  329:Vacuum 312:  252:vacuum 241:outgas 36:, but 547:Gases 369:(PDF) 231:or a 178:ULVAC 91:gases 504:ISBN 468:ISSN 345:ISSN 310:ISSN 209:Torr 93:and 460:doi 337:doi 302:doi 254:). 174:IBM 114:or 538:: 502:. 466:. 458:. 446:. 422:11 420:, 416:, 343:. 333:37 331:. 308:. 296:. 248:Pa 196:, 110:, 81:A 512:. 474:. 462:: 454:: 448:3 428:: 351:. 339:: 316:. 304:: 298:8 180:( 72:) 66:( 61:) 57:( 43:.

Index

references
inline citations
improve
introducing
Learn how and when to remove this message
vacuum pump
gases
vapours
diffusion pump
McLeod gauge
supercooling
hydrogen
kelvins
activated charcoal
liquid helium
cryocoolers
Arthur D. Little Inc.
Howard O. McMahon
Gifford-McMahon cryocooler
IBM
ULVAC
jp:アルバック
dry ice
liquid nitrogen
cryocooler
Torr
sorption pumps
activated charcoal
zeolite
sorbent

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