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75:) offered in certain models can now produce working temperatures up to 1800 °C. This facilitates more sophisticated applications. Common material for the reaction tubes include
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interface, and permit the operator to program segments for uses like ramping, soaking, sintering, and more. Advanced materials in the heating elements, such as
193:
J. D. Corbett "Synthesis of Solid-State
Materials" in Solid State Chemistry: Techniques, A. K. Cheetham and P. Day, Eds. Clarendon, Oxford, 1987.
147:, in the appropriate molar ratio, contained in a platinum or alumina "boat," is heated in a tube furnace at several hundred degrees under flowing
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159:. Because of the availability of tube furnaces, chemical vapor transport has become a popular technique not only in industry (see
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often utilize a fused quartz tube, usually packed with quartz or ceramic beads, which is heated at high temperatures.
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The tube furnace was invented in the first decade of the 20th century and was originally used to manufacture
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is prepared in a tube furnace followed by purification, also in a tube furnace using the technique of
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reactions, involving either organic or inorganic reactants. One such example is the preparation of
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213:"On a New Type of Electric Furnace, with a Redetermination of the Melting-Point of Platinum"
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that are embedded in a thermally insulating matrix. Temperature can be controlled via
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255:) and Its Intercalation Compounds" Inorganic Syntheses 1995, volume 30, pp. 155.
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An example of a material prepared using a tube furnace is the
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which may employ a tube furnace in the 'ketene lamp'.
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device used to conduct syntheses and purifications of
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23:Tube furnace being used during synthesis of
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163:) but also in the research laboratory.
87:, or in the case of corrosive materials
251:J. F. Revelli, "Tantalum Disulfide (TaS
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7:
166:Tube furnaces can also be used for
217:Proceedings of the Royal Society A
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211:Harker, J. A. (December 1905).
1:
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261:10.1002/9780470132616.ch32
161:van Arkel–de Boer process
117:Illustrative applications
157:chemical vapor transport
27:using HCl and aluminium
16:Electric heating device
238:10.1098/rspa.1905.0023
176:Flash vacuum pyrolysis
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69:molybdenum disilicide
61:transport experiments
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283:Laboratory equipment
43:and occasionally in
229:1905RSPSA..76..235H
95:tubes can be used.
41:inorganic compounds
153:tantalum disulfide
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25:aluminium chloride
45:organic synthesis
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223:(507): 235–249.
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151:. Similarly
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107:Nernst lamps
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85:fused quartz
57:thermocouple
33:tube furnace
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168:thermolysis
272:Categories
182:References
89:molybdenum
103:filaments
278:Furnaces
93:tungsten
53:feedback
225:Bibcode
172:ketenes
111:glowers
100:ceramic
77:alumina
55:from a
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149:oxygen
83:, and
65:RS-232
35:is an
288:Kilns
81:Pyrex
71:(MoSi
195:ISBN
109:and
105:for
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126:YBa
91:or
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130:Cu
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31:A
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145:3
143:O
141:2
136:7
134:O
132:3
128:2
73:2
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