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698:"The Preparation of 3:5-Dinitrobenzoic Acid and 3:5-Dinitrobenzoyl Chloride – Observations on the Acylation of Amino-acids by means of 3:5-Dinitrobenzoyl Chloride and certain other Acid Chlorides"
471:
92:
590:
463:
610:. It is used in cases where the substance to be analyzed is sensitive and cannot be directly reacted with 3,5-dinitrobenzoic acid. Generally, the reaction is done in
287:
467:
793:
665:
W. T. Robinson, R. H. Cundiff, P. C. Markunas: „Rapid
Determination of Organic Hydroxyl Groups with 3,5-Dinitrobenzoyl Chloride“, in:
824:
801:
262:
778:
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205:
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3,5-Dinitrobenzoyl chloride has its main use in the analysis of organic compounds by derivatization, specifically of
162:
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459:
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150:
570:
112:
427:
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773:(in German) (19th ed.). Leipzig·Berlin·Heidelberg: Johann Ambrosius Barth. 1993. p. 424.
749:(in German) (19th ed.). Leipzig·Berlin·Heidelberg: Johann Ambrosius Barth. 1993. p. 440.
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via reaction with 3,5-dinitrobenzoyl chloride. The product has a melting point of 177 °C
561:
3,5-dinitrobenzoyl chloride is prepared by the reaction of 3,5-dinitrobenzoic acid with
483:
247:
154:
68:
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released. With this method, it is for instance possible to identify amino acids.
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and like it is mainly used in the analysis of organic substances by
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Except where otherwise noted, data are given for materials in their
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271:
InChI=1S/C7H3ClN2O5/c8-7(11)4-1-5(9(12)13)3-6(2-4)10(14)15/h1-3H
231:
794:
CRC Handbook of Tables for
Organic Compound Identification
696:
Saunders, B. C.; Stacey, G. J.; Wilding, I. G. E. (1942).
537:) is an organic compound with a melting point of 68–69
365:68–69 °C (154–156 °F; 341–342 K)
193:
569:. It can likewise be prepared by reaction with
67:
375:196 °C (385 °F; 469 K) 11 mmHg
8:
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274:Key: NNOHXABAQAGKRZ-UHFFFAOYSA-N
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22:
503:(at 25 °C , 100 kPa).
679: (8), S. 1030–1034 (
337:
316:
295:C1=C(C=C(C=C1(=O))(=O))C(=O)Cl
1:
656:. Retrieved on 12. März 2017.
17:3,5-Dinitrobenzoyl chloride
654:3,5-Dinitrobenzoyl chloride
519:3,5-Dinitrobenzoyl chloride
45:3,5-Dinitrobenzoyl chloride
29:3,5-Dinitrobenzoyl chloride
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34:
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825:Nitrobenzene derivatives
563:phosphorus pentachloride
442:Precautionary statements
796:, Third Edition, 1984,
681:doi:10.1021/ac60176a050
547:3,5-dinitrobenzoic acid
632:
571:phosphorus trichloride
626:
614:in order to bind the
41:Preferred IUPAC name
355: g·mol
18:
633:
627:Identification of
507:Infobox references
16:
715:10.1042/bj0360368
650:Sigma-Aldrich Co.
616:hydrogen chloride
515:Chemical compound
513:
512:
428:Hazard statements
227:CompTox Dashboard
93:Interactive image
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709:(3–4): 368–375.
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579:thionyl chloride
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551:derivatization
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501:standard state
498:
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472:P305+P351+P338
464:P303+P361+P353
460:P301+P330+P331
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802:0-8493-0303-6
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145:ECHA InfoCard
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541:. It is the
518:
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419:
386:
52:Identifiers
703:Biochem. J.
668:Anal. Chem.
414:Signal word
304:Properties
151:100.002.500
814:Categories
780:3335003438
756:3335003438
638:References
398:Pictograms
348:Molar mass
215:5JFA2DVM4D
124:ChemSpider
80:3D model (
59:CAS Number
771:Organikum
747:Organikum
557:Synthesis
468:P304+P340
389:labelling
172:202-750-6
164:EC Number
733:16747534
612:pyridine
604:alcohols
380:Hazards
724:1265703
629:alanine
182:PubChem
69:99-33-2
800:
777:
753:
731:
721:
608:amines
581:, SOCl
420:Danger
353:230.56
288:SMILES
104:ChEMBL
35:Names
577:, or
573:, PCl
565:, PCl
263:InChI
82:JSmol
798:ISBN
775:ISBN
751:ISBN
729:PMID
673:1961
606:and
598:Uses
492:P501
488:P405
484:P363
480:P321
476:P310
456:P280
452:P264
448:P260
434:H314
206:UNII
195:7432
133:7154
719:PMC
711:doi
545:of
529:ClN
387:GHS
232:EPA
185:CID
816::
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717:.
707:36
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677:33
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671:,
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539:°C
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567:5
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525:H
523:7
341:5
338:O
335:2
332:N
326:3
323:H
320:7
317:C
234:)
230:(
84:)
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