1174:
380:
369:
were obtained in 1950 by
Glemser and Lutz, by ambient-temperature reactions. The hydrogen in these compounds can be replaced by alkali metals by treatment with solutions of the corresponding halides. Reactions are conducted in an
1376:
Martha
Greenblatt (1996), "Molybdenum and tungsten bronzes: Low-dimensional metals with unisial properties". In C. Schlenker ed., "Physics and Chemistry of Low-Dimensional Inorganic Conductors" Book, Springer, 481 pages.
1719:
E. Canadell and M.-H. Wangbo (1996), "Fermi surfaces instabilities in oxides and bronzes". In C. Schlenker ed. (1996), "Physics and
Chemistry of Low-Dimensional Inorganic Conductors" Book, Springer, 481 pages.
113:. These compounds form deeply coloured plate-like crystals with a metallic sheen, hence their name. These bronzes derive their metallic character from partially occupied 4d bands. The oxidation states in K
305:
Another preparation technique involves crystallization from the melt in a temperature gradient. This report also called attention to the marked anisotropic resistivity of the purple lithium bronze
290:
and 560 °C, respectively. Sodium bronzes were also obtained by the same method. It was observed that at a slightly higher temperature (about 575 °C and above) only
1795:
Ramanujachary, K.V.; Greenblatt, D.M.; Jones, E.B.; McCarroll, W.H. (1993). "Synthesis and
Characterization of a New Modification of the Quasi-Low-Dimensional Compound KMo
1846:
Andrade, Margareth; Maffei, Mariana
Lanzoni; Alves, Leandro Marcos Salgado; Santos, Carlos Alberto Moreira dos; Ferreira, Bento; Sartori, Antonio Fernando (2012-10-11).
1394:
Greenblatt, M.; McCarroll, W.H.; Neifeld, R.; Croft, M.; Waszczak, J.V. (1984). "Quasi two-dimensional electronic properties of the lithium molybdenum bronze, Li
211:. The first unambiguous synthesis of alkali molybdenum bronzes was reported only in 1964, by Wold and others. They obtained two potassium bronzes, "red"
1895:
Alves, L. M. S.; Damasceno, V. I.; dos Santos, C. A. M.; Bortolozo, A. D.; Suzuki, P. A.; Izario Filho, H. J.; Machado, A. J. S.; Fisk, Z. (2010-05-26).
1960:
1339:
Wold, A.; Kunnmann, W.; Arnott, R. J.; Ferretti, A. (1964). "Preparation and
Properties of Sodium and Potassium Molybdenum Bronze Crystals".
1512:
Chin, Kin; Eda, Kazuo; Sotani, Noriyuki; Whittingham, M.Stanley (2002). "Hydrothermal
Synthesis of the Blue Potassium Molybdenum Bronze, K
1669:
Collins, B.T.; Ramanujachary, K.V.; Greenblatt, M.; Waszczak, J.V. (1985). "Charge-density wave instability and nonlinear transport in Tl
1109:
Other molybdenum bronzes with anomalous electrical properties have been reported, which do not fit in these families. These include
148:
The first report of a "molybdenum bronze" was by Alfred
Stavenhagen and E. Engels in 1895. They reported that electrolysis of molten
1725:
1382:
1965:
974:
797:
1002:
1955:
865:
933:
899:
1058:
654:
137:
831:
734:
709:
560:
480:
1030:
454:
336:
535:
1234:
Onoda, M.; Toriumi, K.; Matsuda, Y.; Sato, M. (1987). "Crystal structure of lithium molybdenum purple bronze Li
1209:
136:
can vary considerably depending on the direction, in some cases by 200:1 or more. They are generally
1908:
1812:
1761:
1686:
1626:
Whangbo, M. H.; Schneemeyer, L. F. (1986). "Band electronic structure of the molybdenum blue bronze A
1587:
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1271:
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1769:
1744:
Birtill, J.J.; Dickens, P.G. (1979). "Thermochemistry of hydrogen molybdenum bronze phases H
1694:
1643:
1595:
1537:
1469:
1423:
1348:
1302:
1263:
1570:
Tsai, P.P.; Potenza, J.A.; Greenblatt, M.; Schugar, H.J. (1986). "Crystal structure of Li
1912:
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1465:
1419:
1259:
17:
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1949:
1936:
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1599:
1427:
1267:
970:
The hydrogen molybdenum bronzes have similar appearances but different compositions:
1872:
1847:
1489:
94:
1896:
133:
129:
46:
1920:
1452:
Glemser, Oskar; Lutz, Gertrud (1950). "Über ein
Hydroxydhydrid des Molybdäns".
181:
gave indigo-blue needles with metallic sheen, which they analysed by weight as
1306:
1113:
50:
1928:
1897:"Unconventional metallic behavior and superconductivity in the K-Mo-O system"
1881:
1832:
1781:
1706:
1655:
1607:
1549:
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1360:
1314:
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128:
These compounds have been much studied since the 1980s due to their markedly
371:
106:
38:
31:
1824:
1541:
132:
electrical properties, reflecting their layered structure. The electrical
110:
90:
1848:"Microstructure and metal-insulator transition in single crystalline KMo
1647:
1352:
379:
1473:
287:
98:
651:. Their electronic properties generally do not depend on the metal A.
340:
102:
1290:
378:
794:. Their electronic properties depend strongly on the metal A.
1168:
1578:, a stoichiometric, triclinic, lithium molybdenum bronze".
402:
Molybdenum bronzes are classified in three major families:
34:, a form of bronze which takes on a purple-colored patina.
1460:(23). Springer Science and Business Media LLC: 539–540.
30:"Purple bronze" redirects here. Not to be confused with
1184:
27:
Generic name for certain mixed oxides of molybdenum
1642:(14). American Chemical Society (ACS): 2424–2429.
391:, also called "potassium-molybdenum blue bronze".
140:. Some are metals and some are semiconductors.
1907:(17). American Physical Society (APS): 174532.
1347:(4). American Chemical Society (ACS): 545–547.
1295:Berichte der Deutschen Chemischen Gesellschaft
8:
975:Hydrogen molybdenum orthorhombic blue bronze
1372:
1370:
125:is an insulator, with an unfilled 4d band.
1739:
1737:
1735:
1733:
1621:
1619:
1617:
1003:Hydrogen molybdenum monoclinic blue bronze
1871:
1447:
1445:
1229:
1227:
1225:
1221:
1212: – Chemical intercalation compound
1565:
1563:
1561:
1559:
1507:
1505:
1503:
1501:
1499:
1334:
1332:
1330:
1328:
1326:
1324:
1677:a new blue molybdenum oxide bronze".
7:
1866:(6). FapUNIFESP (SciELO): 998–1002.
1289:Stavenhagen, A.; Engels, E. (1895).
866:Potassium molybdenum purple bronze
764:, generally with limiting formula
25:
1165:Electrical and thermal properties
934:Thallium molybdenum purple bronze
900:Rubidium molybdenum purple bronze
1805:Journal of Solid State Chemistry
1754:Journal of Solid State Chemistry
1580:Journal of Solid State Chemistry
1522:Journal of Solid State Chemistry
1248:Journal of Solid State Chemistry
1172:
1059:Hydrogen molybdenum green bronze
798:Lithium molybdenum purple bronze
655:Potassium molybdenum blue bronze
1873:10.1590/s1516-14392012005000132
832:Sodium molybdenum purple bronze
735:Thallium molybdenum blue bronze
710:Rubidium molybdenum blue bronze
561:Potassium molybdenum red bronze
481:Potassium molybdenum red bronze
1685:(12). Elsevier BV: 1023–1028.
1031:Hydrogen molybdenum red bronze
45:is a generic name for certain
1:
455:Lithium molybdenum red bronze
337:metal-to-insulator transition
1961:Non-stoichiometric compounds
1774:10.1016/0022-4596(79)90193-2
1699:10.1016/0038-1098(85)90863-4
1600:10.1016/0022-4596(86)90120-9
1428:10.1016/0038-1098(84)90944-x
1268:10.1016/0022-4596(87)90231-3
600:, with limiting composition
536:Cesium molybdenum red bronze
253:, by electrolysis of molten
138:non-stoichiometric compounds
1760:(3). Elsevier BV: 367–372.
1414:(9). Elsevier BV: 671–674.
1254:(1). Elsevier BV: 163–170.
1982:
1921:10.1103/physrevb.81.174532
1679:Solid State Communications
1408:Solid State Communications
409:with limiting composition
29:
1811:(1). Elsevier BV: 69–78.
1586:(1). Elsevier BV: 47–56.
1528:(1). Elsevier BV: 81–87.
1307:10.1002/cber.189502802213
53:with the generic formula
1055:, 1.55 < x < 1.72
18:Molybdenum purple bronze
1966:Transition metal oxides
1454:Die Naturwissenschaften
1301:(2). Wiley: 2280–2281.
1291:"Ueber Molybdänbronzen"
1027:, 0.85 < x < 1.4
999:, 0.23 < x < 0.4
1825:10.1006/jssc.1993.1008
1542:10.1006/jssc.2001.9450
1210:Sodium tungsten bronze
1181:This section is empty.
392:
374:at about 160 °C.
121:are K, O, and Mo. MoO
382:
1956:Molybdenum compounds
1913:2010PhRvB..81q4532A
1817:1993JSSCh.102...69R
1766:1979JSSCh..29..367B
1691:1985SSCom..56.1023C
1648:10.1021/ic00234a028
1636:Inorganic Chemistry
1592:1986JSSCh..64...47T
1534:2002JSSCh.164...81C
1466:1950NW.....37..539G
1420:1984SSCom..51..671G
1353:10.1021/ic50014a022
1341:Inorganic Chemistry
1260:1987JSSCh..66..163O
1860:Materials Research
1474:10.1007/bf00589341
393:
1901:Physical Review B
1201:
1200:
592:a semi-conductor.
346:Hydrogen bronzes
43:molybdenum bronze
16:(Redirected from
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89:where A may be
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1634:(A = K, Rb)".
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762:Purple bronzes
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1471:
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1456:(in German).
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1350:
1346:
1342:
1335:
1333:
1331:
1329:
1327:
1325:
1321:
1316:
1312:
1308:
1304:
1300:
1296:
1292:
1285:
1282:
1277:
1273:
1269:
1265:
1261:
1257:
1253:
1249:
1230:
1228:
1226:
1222:
1216:
1211:
1208:
1207:
1203:
1195:
1186:
1182:
1178:
1175:
1171:
1170:
1164:
1146:
1137:
1115:
1112:
1111:
1110:
1060:
1057:
1041:
1032:
1029:
1013:
1004:
1001:
985:
976:
973:
972:
971:
935:
932:
901:
898:
867:
864:
833:
830:
799:
796:
795:
763:
760:
736:
733:
711:
708:
656:
653:
652:
599:
596:
562:
559:
537:
534:
482:
479:
456:
453:
452:
408:
405:
404:
403:
397:
383:Crystals of K
381:
377:
376:
375:
373:
355:
344:
342:
338:
303:
302:is obtained.
289:
143:
141:
139:
135:
131:
126:
112:
108:
104:
100:
96:
92:
84:
73:
62:
52:
48:
44:
40:
33:
19:
1904:
1900:
1890:
1863:
1859:
1841:
1808:
1804:
1790:
1757:
1753:
1715:
1682:
1678:
1664:
1639:
1635:
1583:
1579:
1525:
1521:
1457:
1453:
1411:
1407:
1389:
1344:
1340:
1298:
1294:
1284:
1251:
1247:
1189:
1185:adding to it
1180:
1144:
1108:
1039:
1011:
983:
969:
761:
598:Blue bronzes
597:
406:
401:
353:
345:
339:at about 24
304:
147:
127:
95:alkali metal
82:
71:
60:
47:mixed oxides
42:
36:
621:, that is,
430:, that is,
407:Red bronzes
232:and "blue"
144:Preparation
134:resistivity
130:anisotropic
1950:Categories
1217:References
1192:March 2020
1114:Tetragonal
51:molybdenum
1937:123147025
1929:1098-0121
1882:1980-5373
1833:0022-4596
1782:0022-4596
1707:0038-1098
1656:0020-1669
1608:0022-4596
1550:0022-4596
1482:0028-1042
1436:0038-1098
1361:0020-1669
1315:0365-9496
1276:0022-4596
372:autoclave
39:chemistry
32:Hepatizon
1490:46699509
1204:See also
335:and its
91:hydrogen
1909:Bibcode
1813:Bibcode
1762:Bibcode
1687:Bibcode
1588:Bibcode
1530:Bibcode
1462:Bibcode
1416:Bibcode
1256:Bibcode
286:at 550
109:), and
1935:
1927:
1880:
1831:
1780:
1724:
1705:
1654:
1606:
1548:
1488:
1480:
1434:
1381:
1359:
1313:
1274:
1933:S2CID
1486:S2CID
93:, an
1925:ISSN
1878:ISSN
1829:ISSN
1778:ISSN
1722:ISBN
1703:ISSN
1652:ISSN
1628:0.30
1604:ISSN
1572:0.33
1546:ISSN
1514:0.28
1478:ISSN
1432:ISSN
1379:ISBN
1357:ISSN
1311:ISSN
1272:ISSN
672:1.02
663:0.28
607:0.30
578:1.01
569:0.23
544:0.33
498:1.02
489:0.26
463:0.33
416:0.33
385:0.28
239:0.28
218:0.26
169:and
115:0.28
1917:doi
1868:doi
1821:doi
1809:102
1803:".
1770:doi
1752:".
1748:MoO
1695:doi
1673:MoO
1671:0.3
1644:doi
1630:MoO
1596:doi
1574:MoO
1538:doi
1526:164
1520:".
1516:MoO
1470:doi
1424:doi
1406:".
1396:0.9
1349:doi
1303:doi
1264:doi
1246:".
1236:0.9
1187:.
1155:2−δ
1150:MoO
1117:KMo
1083:MoO
1081:or
1071:MoO
1045:MoO
1017:MoO
989:MoO
942:0.9
908:0.9
874:0.9
840:0.9
806:0.9
771:0.9
747:MoO
743:0.3
722:MoO
718:0.3
697:MoO
693:0.3
686:or
611:MoO
548:MoO
523:MoO
519:0.3
512:or
467:MoO
432:AMo
420:MoO
387:MoO
359:MoO
312:0.9
292:MoO
276:MoO
264:MoO
243:MoO
222:MoO
171:MoO
159:MoO
117:MoO
49:of
37:In
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1297:.
1293:.
1270:.
1262:.
1252:66
1250:.
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1224:^
960:17
946:Mo
937:Cs
926:17
912:Mo
903:Rb
892:17
878:Mo
858:17
844:Mo
835:Na
824:17
810:Mo
801:Li
789:17
775:Mo
738:Tl
713:Rb
667:Mo
646:30
637:10
632:Mo
573:Mo
539:Cs
493:Mo
458:Li
451::
343:.
330:17
316:Mo
307:Li
288:°C
192:Mo
183:Na
150:Na
111:Tl
105:,
103:Na
101:,
99:Li
66:Mo
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1919::
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1266::
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1190:(
1160:.
1145:x
1139:K
1131:6
1126:O
1122:4
1104:O
1100:2
1095:H
1093:.
1088:2
1076:3
1067:2
1062:H
1050:3
1040:x
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1022:3
1012:x
1006:H
994:3
984:x
978:H
955:O
951:6
921:O
917:6
887:O
883:6
869:K
853:O
849:6
819:O
815:6
784:O
780:6
766:A
752:3
727:3
702:3
688:K
681:3
676:O
658:K
641:O
628:3
623:A
616:3
602:A
587:3
582:O
564:K
553:3
528:3
514:K
507:3
502:O
484:K
472:3
446:9
441:O
437:3
425:3
411:A
389:3
364:3
354:x
348:H
341:K
325:O
321:6
297:2
281:3
274:+
269:4
260:2
255:K
248:3
234:K
227:3
213:K
206:7
201:O
197:5
188:2
176:3
164:4
155:2
123:3
119:3
107:K
83:z
77:O
72:y
61:x
55:A
20:)
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