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specifically when recording absorbance readings from
Ultraviolet-visible Spectroscopy, since thicker films have lower optical transmittance and typically do not allow light to shine through in comparison to thinner films allowing light to go through before the optical density of the film becomes too low. Additionally, films with lower absorbance quality are not as ideal of candidates for processes such as Cyclic Voltammetry because the low absorbance hinders electrochemical tuning of cations when in an electrochemical cell. Thinner films in this regard have more desirable optical properties that can be tuned for energy storage technologies because of their spin coated influenced properties. However, spin coating thicker films of
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of the solution, and the solvent. Pioneering theoretical analysis of spin coating was undertaken by Emslie et al., and has been extended by many subsequent authors (including Wilson et al., who studied the rate of spreading in spin coating; and
Danglad-Flores et al., who found a universal description
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One advantage to spin coating thin films is the uniformity of the film thickness. Owing to self-leveling, thicknesses do not vary more than 1%. The thickness of films produced in this manner may also affect the optical properties of such materials. This is important for electrochemical testing,
50:. Usually a small amount of coating material in liquid form is applied on the center of the substrate, which is either spinning at low speed or not spinning at all. The substrate is then rotated at speeds up to 10,000 rpm to spread the coating material by
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thick. Photoresist is typically spun at 20 to 80 revolutions per second for 30 to 60 seconds. It is also widely used for the fabrication of planar photonic structures made of polymers.
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Rotation is continued while the fluid spins off the edges of the substrate, until the desired thickness of the film is achieved. The applied solvent is usually
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Schubert, Dirk W.; Dunkel, Thomas (2003). "Spin coating from a molecular point of view: its concentration regimes, influence of molar mass and distribution".
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Hanaor, D.A.H.; Triani, G.; Sorrell, C.C. (2011). "Morphology and photocatalytic activity of highly oriented mixed phase titanium dioxide thin films".
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S. Middleman and A.K. Hochberg. "Process
Engineering Analysis in Semiconductor Device Fabrication". McGraw-Hill, p. 313 (1993)
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precursors, where it can be used to create uniform thin films with nanoscale thicknesses. It is used intensively in
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Emslie, A. G.; Bonner, F. T.; Peck, L. G. (1958). "Flow of a viscous liquid on a rotating disk".
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Wilson, S. K.; Hunt, R.; Duffy, B. R. (2000). "The rate of spreading in spin coating".
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Scriven, L. E. (1988). "Physics and
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can result in relatively large edge beads whose planarization has physical limits.
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Deposition of polymer films by spin casting: A quantitative analysis
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Cohen, Edward; Lightfoot, E. J. (2011). "Coating
Processes".
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Danglad-Flores, J.; Eickelmann, S.; Riegler, H. (2018).
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501:Spin Coating of Thin and Ultrathin Polymer Films
140:Kirk-Othmer Encyclopedia of Chemical Technology
407:Journal of Micromechanics and Microengineering
54:. A machine used for spin coating is called a
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335:(12). Elsevier BV: 3658–3664.
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142:. New York: John Wiley.
401:Arscott, Steve (2020).
381:"What Is Spin Coating?"
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